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ASTM E350-23

Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron

Summary

1.1 These test methods cover the chemical analysis of carbon steels, low-alloy steels, silicon electrical steels, ingot iron, and wrought iron having chemical compositions within the following limits:

Element

?Composition Range,?%

Aluminum

0.001? to 1.50

Antimony

0.002? to 0.03

Arsenic

0.0005 to 0.10

Bismuth

0.005? to 0.50

Boron

0.0005 to 0.02

Calcium

0.0005 to 0.01

Cerium

0.005? to 0.50

Chromium

0.005? to 3.99

Cobalt

0.01?? to 0.30

Columbium (Niobium)

0.002? to 0.20

Copper

0.005? to 1.50

Lanthanum

0.001? to 0.30

Lead

0.001? to 0.50

Manganese

0.01?? to 2.50

Molybdenum

0.002? to 1.50

Nickel

0.005? to 5.00

Nitrogen

0.0005 to 0.04

Oxygen

0.0001 to 0.03

Phosphorus

0.001? to 0.25

Selenium

0.001? to 0.50

Silicon

0.001? to 5.00

Sulfur

0.001? to 0.60

Tin

0.002? to 0.10

Titanium

0.002? to 0.60

Tungsten

0.005? to 0.10

Vanadium

0.005? to 0.50

Zirconium

0.005? to 0.15

1.2 The test methods in this standard are contained in the sections indicated as follows:

 

Sections

 

 

Aluminum, Total, by the 8-Quinolinol Gravimetric
?Method (0.20?% to 1.5?%)

124131

Aluminum, Total, by the 8-Quinolinol
?Spectrophotometric Method
?(0.003?% to 0.20?%)

7686

Aluminum, Total or Acid-Soluble, by the Atomic
?Absorption?Spectrometry Method
?(0.005?% to 0.20?%)

308317

Antimony by the Brilliant Green Spectrophotometric
?Method (0.0002?% to 0.030?%)

142151

Bismuth by the Atomic Absorption Spectrometry
?Method (0.02?% to 0.25?%)

298307

Boron by the Distillation-Curcumin
?Spectrophotometric Method
?(0.0003?% to 0.006?%)

208219

Calcium by the Direct-Current Plasma Atomic
?Emission Spectrometry Method
?(0.0005?% to 0.010?%)

289297

Carbon, Total, by the Combustion Gravimetric Method
?(0.05?% to 1.80?%)—Discontinued 1995

 

Cerium and Lanthanum by the Direct Current Plasma
?Atomic Emission Spectrometry Method
?(0.003?% to 0.50?% Cerium, 0.001?% to 0.30?%
?Lanthanum)

249257

Chromium by the Atomic Absorption Spectrometry
?Method (0.006?% to 1.00?%)

220229

Chromium by the Peroxydisulfate Oxidation-Titration
?Method (0.05?% to 3.99?%)

230238

Cobalt by the Nitroso-R Salt Spectrophotometric
?Method (0.01?% to 0.30?%)

5362

Copper by the Sulfide Precipitation-Iodometric
?Titration Method (Discontinued 1989)

8794

Copper by the Atomic Absorption Spectrometry
?Method (0.004?% to 0.5?%)

279288

Copper by the Neocuproine Spectrophotometric
?Method (0.005?% to 1.50?%)

114123

Lead by the Ion-Exchange—Atomic Absorption
?Spectrometry Method
?(0.001?% to 0.50?%)

132141

Manganese by the Atomic Absorption Spectrometry
?Method (0.005?% to 2.0?%)

269278

Manganese by the Metaperiodate Spectrophotometric
?Method (0.01?% to 2.5?%)

918

Manganese by the Peroxydisulfate-Arsenite Titrimetric
?Method (0.10?% to 2.50?%)

164171

Molybdenum by the Thiocyanate Spectrophotometric
?Method (0.01?% to 1.50?%)

152163

Nickel by the Atomic Absorption Spectrometry
?Method (0.003?% to 0.5?%)

318327

Nickel by the Dimethylglyoxime Gravimetric
?Method (0.1?% to 5.00?%)

180187

Nickel by the Ion-Exchange-Atomic-Absorption
?Spectrometry Method
?(0.005?% to 1.00?%)

188197

Nitrogen by the Distillation-Spectrophotometric
?Method (Discontinued 1988)

6375

Phosphorus by the Alkalimetric Method
?(0.02?% to 0.25?%)

172179

Phosphorus by the Molybdenum Blue
?Spectrophotometric Method
?(0.003?% to 0.09?%)

1930

Silicon by the Molybdenum Blue Spectrophotometric
?Method (0.01?% to 0.06?%)

103113

Silicon by the Gravimetric Titration
?Method (0.05?% to 3.5?%)

4652

Sulfur by the Gravimetric Method
?(Discontinued 1988)

3136

Sulfur by the Combustion-Iodate Titration Method
?(0.005?% to 0.3?%) (Discontinued 2017)

3745

Tin by the Sulfide Precipitation-Iodometric Titration
?Method (0.01?% to 0.1?%)

95102

Tin by the Solvent Extraction-Atomic Absorption
?Spectrometry Method
?(0.002?% to 0.10?%)

198207

Titanium by the Diantipyrylmethane
?Spectrophotometric Method
?(0.025?% to 0.30?%)

258268

Vanadium by the Atomic Absorption Spectrometry
?Method (0.006?% to 0.15?%)

239248

1.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E1019.

1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in IEEE/ASTM SI 10 are also used.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special “Warning” paragraphs throughout these test methods.

1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Significance and Use:

4.1 These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of ASTM Committees A01 on Steel, Stainless Steel, and Related Alloys and A04 on Iron Castings. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.

Technical characteristics

Publisher American Society for Testing and Materials (ASTM International)
Publication Date 11/15/2023
Collection
Page Count 64
Themes Chemical analysis of metals
EAN ---
ISBN ---
Weight (in grams) ---