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ISO 18363-3:2024

Animal and vegetable fats and oils
Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS

Summary

ISO 18363 specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3-MCPD esters (bound 3-MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis. ISO 18363-3 is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.

Notes

50.60 : Clôture du vote Epreuve retournée par le secrétariat

Technical characteristics

Publisher International Organization for Standardization (ISO)
Publication Date 07/01/2024
Edition 2
Page Count 17
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ISBN ---
Weight (in grams) ---